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Ring annulation versus alkylation of pyrrole with alpha-phosphoryl-alpha,beta-unsaturated ketones

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2016

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Pergamon-Elsevier Science LTD

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Abstract

In this study; novel aryl, heteroaryl, pyrrolyl and phosphoryl groups containing pyrrolizines were synthesized by the ring annulation reaction of aryl or heteroaryl substituted alpha-phosphoryl-alpha,beta-unsaturated ketones with pyrrole under mild reaction conditions. This domino reaction involves scandium triflate catalyzed addition of pyrrole to the double bond of alpha-phosphoryl-alpha,beta-unsaturated ketones, carbonyl group and finally ring annulation sequences. The presented work provided a convenient way for the synthesis of novel bispyrrolic compounds. (C) 2016 Elsevier Ltd. All rights reserved.

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Keywords

Pyrrolizines, Phosphonates, Ring Annulation, Michael Addition

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Citation

Tasgin, Dilek Isik; Unaleroglu, Canan, "Ring annulation versus alkylation of pyrrole with alpha-phosphoryl-alpha,beta-unsaturated ketones", Tetrahedron, Vol. 72, No. 39, pp. 5934-5942, (2016).

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Tetrahedron

Volume

72

Issue

39

Start Page

5934

End Page

5942